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The interaction of different metals acetylacetonates with a supramolecular polymer is demonstrated by X-ray diffraction, infrared spectroscopy, and microspectrophotometric measurements. The supramolecular polymer catechol-formaldehyde (CFO) acts as a stabilizing template in the formation of two new supramolecular coordination polymers of Mn(2+), Zn(2+), Ni(2+), and Cd(2+) with a metal/ligand ratio of 1/1. The crystal structures of the nickel and cadmium complexes are assigned as 1D coordination polymers (Ni-APAC, 1, Ni(2+)-N(3), and Cd-APAC, 2). These polymeric materials are formed by the self-assembly of CFO molecules and acetylacetonate complexes, which are connected via hydrogen bonds. The polymeric assembly shows remarkable thermal stability due to hydrogen bonds in the solid state. Therefore, the electronic structures of the polymeric complexes of Mn, Zn, Ni, and Cd have been studied by microspectrophotometric measurements. return { 0b46394aab